158 research outputs found
Two-Dimensional Magnetic Resonance Tomographic Microscopy using Ferromagnetic Probes
We introduce the concept of computerized tomographic microscopy in magnetic
resonance imaging using the magnetic fields and field gradients from a
ferromagnetic probe. We investigate a configuration where a two-dimensional
sample is under the influence of a large static polarizing field, a small
perpendicular radio-frequency field, and a magnetic field from a ferromagnetic
sphere. We demonstrate that, despite the non-uniform and non-linear nature of
the fields from a microscopic magnetic sphere, the concepts of computerized
tomography can be applied to obtain proper image reconstruction from the
original spectral data by sequentially varying the relative sample-sphere
angular orientation. The analysis shows that the recent proposal for atomic
resolution magnetic resonance imaging of discrete periodic crystal lattice
planes using ferromagnetic probes can also be extended to two-dimensional
imaging of non-crystalline samples with resolution ranging from micrometer to
Angstrom scales.Comment: 9 pages, 11 figure
Pervasive melt percolation reactions in ultra-depleted refractory harzburgites at the Mid-Atlantic Ridge, 15° 20′N : ODP Hole 1274A
Author Posting. © The Authors, 2006. This is the author's version of the work. It is posted here by permission of Springer for personal use, not for redistribution. The definitive version was published in Contributions to Mineralogy and Petrology 153 (2007): 303-319, doi:10.1007/s00410-006-0148-6.ODP Leg 209 Site 1274 mantle peridotites are highly refractory in terms of lack of residual
clinopyroxene, olivine Mg# (up to 0.92) and spinel Cr# (~0.5), suggesting high degree of partial
melting (>20%). Detailed studies of their microstructures show that they have extensively
reacted with a pervading intergranular melt prior to cooling in the lithosphere, leading to
crystallization of olivine, clinopyroxene and spinel at the expense of orthopyroxene. The least
reacted harzburgites are too rich in orthopyroxene to be simple residues of low-pressure (spinel
field) partial melting. Cu-rich sulfides that precipitated with the clinopyroxenes indicate that
the intergranular melt was generated by no more than 12% melting of a MORB mantle or by
more extensive melting of a clinopyroxene-rich lithology. Rare olivine-rich lherzolitic domains,
characterized by relics of coarse clinopyroxenes intergrown with magmatic sulfides, support
the second interpretation. Further, coarse and intergranular clinopyroxenes are highly depleted
in REE, Zr and Ti. A two-stage partial melting/melt-rock reaction history is proposed, in which
initial mantle underwent depletion and refertilization after an earlier high pressure (garnet field)
melting event before upwelling and remelting beneath the present-day ridge. The ultra-depleted
compositions were acquired through melt re-equilibration with residual harzburgites.Funding for this
research was provided by Centre National de la Recherche Scientifique-Institut National des
Sciences de l’Univers (Programme Dynamique et Evolution de la Terre Interne)
Instrumental aspects of magnetic resonance force microscopy
A novel sample preparation technique for deposition of small volumes from the liquid phase is described. Samples with diameters as small as 0.5 mu m were created with this technique. A series of cantilever geometries was manufactured, with the aim of optimizing the e-factor. Force sensitivities of 8 x 10(-17) N/root Hz were achieved at room temperature, which is a considerable improvement over commercial cantilevers. Mechanisms which determine e-factors are discussed briefly. Quantitative understanding of MRFM is absolutely necessary. Calculations of the magnetic field and field gradients for several types of permanent magnets are presented
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